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Phys. Rev. A 75, 032702 (2007) [14 pages]

Measurement of the x-ray mass attenuation coefficient and determination of the imaginary component of the atomic form factor of tin over the energy range of 29–60 keV

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Martin D. de Jonge
X-Ray Operations and Research, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA

Chanh Q. Tran, Christopher T. Chantler, Zwi Barnea, and Bipin B. Dhal
School of Physics, University of Melbourne, Victoria 3010, Australia

David Paterson
Australian Synchrotron Project, Major Projects Victoria, 800 Blackburn Road, Clayton, Victoria 3168, Australia

Elliot P. Kanter, Stephen H. Southworth, and Linda Young
Chemistry Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA

Mark A. Beno, Jennifer A. Linton, and Guy Jennings
BESSRC-CAT, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA

Received 11 September 2006; published 6 March 2007

We use the x-ray extended-range technique (XERT) [ C. T. Chantler et al. Phys. Rev. A 64 062506 (2001)] to measure the mass attenuation coefficients of tin in the x-ray energy range of 29–60 keV to 0.04–3 % accuracy, and typically in the range 0.1–0.2 %. Measurements made over an extended range of the measurement parameter space are critically examined to identify, quantify, and correct a number of potential experimental systematic errors. These results represent the most extensive experimental data set for tin and include absolute mass attenuation coefficients in the regions of x-ray absorption fine structure, extended x-ray absorption fine structure, and x-ray absorption near-edge structure. The imaginary component of the atomic form factor f2 is derived from the photoelectric absorption after subtracting calculated Rayleigh and Compton scattering cross sections from the total attenuation. Comparison of the result with tabulations of calculated photoelectric absorption coefficients indicates that differences of 1–2 % persist between calculated and observed values.

© 2007 The American Physical Society

URL:
http://link.aps.org/doi/10.1103/PhysRevA.75.032702
DOI:
10.1103/PhysRevA.75.032702
PACS:
32.80.Cy, 61.10.Ht, 32.80.Fb, 78.20.Ci